Wikiroot: Created page with "Typical parameters for nmr600: Spectra were acquired on a 600-MHz Inova NMR spectrometer at 25 °C using the tn noesy pulse sequence (circa Vnmr 6.1B software, Varian Inc). ..."

2012-12-18T21:51:21Z

Created page with "Typical parameters for nmr600: Spectra were acquired on a 600-MHz Inova NMR spectrometer at 25 °C using the tn noesy pulse sequence (circa Vnmr 6.1B software, Varian Inc). ..."

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Typical parameters for nmr600:

Spectra were acquired on a 600-MHz Inova NMR spectrometer at 25 °C using the tn noesy pulse sequence (circa Vnmr 6.1B software, Varian Inc).

Spectra had an acquisition time of 4 s, a preacquisition delay of 1 s, a mixing time of 0.1 s, a sweep width of 7200 Hz, and 256 transients.

{Saude, E. J., Slupsky, C. M., and Sykes, B. D. (2006) Metabolomics 2, 113-123}

ACQUISITION SAMPLE PROCESSING 2D PROCESSING
sfrq 599.856 date Sep 29 2010 lb not used lb1 not used
tn H1 solvent D2O sb not used sb1 -0.085
at 4.000 temp 30.0 gf not used sbs1 -0.085
np 67184 DECOUPLING proc ft gf1 not used
sw 8398.1 dn fn 262144 fn1 2048
bs 8 dof -3326.9 ssfilter not used FLAGS
ss 2 dm nnnn ssorder not used dp y
tpwr 58 dmm cccp ssntaps 200 C13refoc n
pw 8.8 dpwr 48 sslsfrq not used N15refoc n
d1 0.010 homo n GRADIENTS CNrefoc n
d2 0 2D ACQUISITION gt1 0.0030 SATURATION
mix 0.100 sw1 8398.1 gzlvl1 5000 mfsat n
tof -219.5 ni 1 gt2 0.0050 sspul n
nt 256 phase 1 gzlvl2 7500 satmode ynyn
ct 256 satpwr 6
satdly 0.990
scuba n

Running NMR spectrum - Revision history

Wikiroot: Created page with "Typical parameters for nmr600: Spectra were acquired on a 600-MHz Inova NMR spectrometer at 25 °C using the tn noesy pulse sequence (circa Vnmr 6.1B software, Varian Inc). ..."