Difference between revisions of "Spectrometers"
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[[Image: Nanuc800.jpg|thumb|right|300px|The Nanuc 800 spectrometer.]] | [[Image: Nanuc800.jpg|thumb|right|300px|The Nanuc 800 spectrometer.]] | ||
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* HONDA generator for extended power failure | * HONDA generator for extended power failure | ||
| − | + | The NANUC 800 is filled with liquid Nitrogen every tuesday on a weekly basis and with liquid Helium every 3 weeks. Weekly data for cryogen levels, flow rates and bath temperatures can be found in the magnet status report. Data on overall magnet stability can be viewed in the monitoring output. | |
| − | + | ||
| − | + | <H2> nmr500 </H2> | |
| − | + | [[Image:nmr500-1.jpg|200px]] [[Image:Flowmeters1.jpg|200px]] | |
| − | + | The nmr 500MHz system was installed on April 26, 1986. The magnet system has a 100L LN2 reservoir. | |
| + | Location: 4-19 MSB | ||
| + | Magnet: 11.7 T Oxford 51mm bore | ||
| − | + | '''Specs''' | |
| + | * Varian INOVA console, | ||
| + | * Z-gradient ONLY, 4 complete channels with Wave Generator Boards, | ||
| + | * (2) 50W Amplifiers, 5.3kVA UPS | ||
| − | + | '''Probes''' | |
| + | * Varian 5mm TRPFG, | ||
| + | * Varian 8mm Biomolecular TRPFG, | ||
| + | * Varian 10mm BB N15-P31 {H1} 50.65 - 202.43 Mhz | ||
| − | + | Local frequency | |
| + | * 1H 499.886376 | ||
| + | * 13C 125.7176027 | ||
| + | * 15N 50.6588595 | ||
| − | + | <B><h2>nmr600</h2></B> | |
| − | + | ||
| − | + | [[Image:nmr600-2.jpg|200px]] [[Image:nmr600-1.jpg|200px]] | |
| − | + | ||
| − | + | ||
| − | + | The nmr 600MHz system was installed in November of 1990. The magnet system has a 155L [[Glossary|LN2]] reservoir. | |
| − | + | ||
| − | + | ||
| − | + | '''Magnet''' | |
| − | + | * 14.09 T Oxford, 51mm bore | |
| − | + | ||
| − | + | ||
| − | + | '''Console''' | |
| + | *Varian INOVA console, Solids/Liquids, | ||
| + | *Z Gradient only, 3 1/2 Channels with Wave Gen Brds, | ||
| + | *1kW BB Amp, 800W HB Amp, 300W BB Amp, 100W HB Amp, 5.3kVA UPS | ||
| − | + | '''Probes''' | |
| − | + | *5mm Triple-resonance PFG probe, | |
| + | *Varian PISEMA (5mm solenoid and 12X10X4mm rectangular coil), Varian 5mm H1/F19, | ||
| + | *Varian 8mm TRPFG, Varian 5mm TR, Varian 3mm F19/H1 PFG UB, | ||
| + | *5mm TRPFG UB, 5mm Indirect Detection | ||
| − | |||
| − | |||
| − | |||
| − | + | <B><h2>ibd600</h2></B> | |
| − | + | ||
| − | + | ||
| − | + | ||
| − | + | [[Image:ibd600-1.jpg|200px]] | |
| − | + | ||
| − | + | ||
| − | + | ||
Latest revision as of 14:01, 20 December 2012
Contents |
NANUC 800 System
The Nanuc 800 was brought online in 2000.
Magnet
- 18.8T 63mm Oxford magnet (2.2K)
Console
- Varian INOVA console
- X, Y, Z gradients
- 4 complete channels with waveform generators
- 1000 W amplifier for 13C (channel #2)
- 1000 W amplifier for 15N (channel #3)
- 400 W amplifier for 2H (channel #4)
Probes
- 5mm HCN - xyz gradient
- 3mm HCN z-gradient (High Salt)
- 5mm Broad Band z-gradient
- 5mm HCN Cold Probe
- MAS T3 HX Balum Solids
Computer & Power
- SUN Ultra-10 with 24"-monitor
- 3kVa UPS for magnet pumps
- 7.5 kVa UPS for console
- HONDA generator for extended power failure
The NANUC 800 is filled with liquid Nitrogen every tuesday on a weekly basis and with liquid Helium every 3 weeks. Weekly data for cryogen levels, flow rates and bath temperatures can be found in the magnet status report. Data on overall magnet stability can be viewed in the monitoring output.
nmr500
The nmr 500MHz system was installed on April 26, 1986. The magnet system has a 100L LN2 reservoir. Location: 4-19 MSB Magnet: 11.7 T Oxford 51mm bore
Specs
- Varian INOVA console,
- Z-gradient ONLY, 4 complete channels with Wave Generator Boards,
- (2) 50W Amplifiers, 5.3kVA UPS
Probes
- Varian 5mm TRPFG,
- Varian 8mm Biomolecular TRPFG,
- Varian 10mm BB N15-P31 {H1} 50.65 - 202.43 Mhz
Local frequency
- 1H 499.886376
- 13C 125.7176027
- 15N 50.6588595
nmr600
The nmr 600MHz system was installed in November of 1990. The magnet system has a 155L LN2 reservoir.
Magnet
- 14.09 T Oxford, 51mm bore
Console
- Varian INOVA console, Solids/Liquids,
- Z Gradient only, 3 1/2 Channels with Wave Gen Brds,
- 1kW BB Amp, 800W HB Amp, 300W BB Amp, 100W HB Amp, 5.3kVA UPS
Probes
- 5mm Triple-resonance PFG probe,
- Varian PISEMA (5mm solenoid and 12X10X4mm rectangular coil), Varian 5mm H1/F19,
- Varian 8mm TRPFG, Varian 5mm TR, Varian 3mm F19/H1 PFG UB,
- 5mm TRPFG UB, 5mm Indirect Detection
ibd600
