Running NMR spectrum

Typical parameters for nmr600:

Spectra were acquired on a 600-MHz Inova NMR spectrometer at 25 °C using the tn noesy pulse sequence (circa Vnmr 6.1B software, Varian Inc).

Spectra had an acquisition time of 4 s, a preacquisition delay of 1 s, a mixing time of 0.1 s, a sweep width of 7200 Hz, and 256 transients.

{Saude, E. J., Slupsky, C. M., and Sykes, B. D. (2006) Metabolomics 2, 113-123}

  ACQUISITION            SAMPLE            PROCESSING        2D PROCESSING
sfrq       599.856  date   Sep 29 2010  lb        not used  lb1       not used
tn              H1  solvent        D2O  sb        not used  sb1         -0.085
at           4.000  temp          30.0  gf        not used  sbs1        -0.085
np           67184      DECOUPLING      proc            ft  gf1       not used
sw          8398.1  dn                  fn          262144  fn1           2048
bs               8  dof        -3326.9  ssfilter  not used        FLAGS
ss               2  dm            nnnn  ssorder   not used  dp               y
tpwr            58  dmm           cccp  ssntaps        200  C13refoc         n
pw             8.8  dpwr            48  sslsfrq   not used  N15refoc         n
d1           0.010  homo             n      GRADIENTS       CNrefoc          n
d2               0    2D ACQUISITION    gt1         0.0030      SATURATION
mix          0.100  sw1         8398.1  gzlvl1        5000  mfsat            n
tof         -219.5  ni               1  gt2         0.0050  sspul            n
nt             256  phase            1  gzlvl2        7500  satmode       ynyn
ct             256                                          satpwr           6
                                                            satdly       0.990
                                                            scuba            n